Six new N-acetylglycine amides and bisamides were prepared by reacting N-acetylglycine with different isocyanates including, hexamethylene diisocyanate, bis(4-isocyanatophenyl)methane, toluene 2,4-diisocyanate, 1,3-bis(2-isocyanatopropan-2-yl)benzene, phenyl isocyanate and 2-naphthyl isocyanate to furnish amides 1-6. The gelation ability of compounds (1-6) was investigated using fourteen different solvents including polar, non-polar organic solvents. Only compound 1 solidified toluene. Characterization of compounds (1-6) was done using spectroscopic methods, HRESI-MS, FTIR, 1H- and 13C-NMR. The morphology of toluene organogel (as xerogel) was determined through scanning electron microscopy (SEM).
Firdous Imran Ali, Rabel Shaikh, Ahmed Bari, Umair Ahmad Khan, Shoaib Muhammad and Imran Ali Hashmi
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